1,3-Dibromopropane / CAS 109-64-8

Name:

1,3-Dibromopropane

Other name:

1,3-propanedibromide

CAS:

109-64-8

Specification:

Molecular formula: C₃H₆Br₂

Molecular weight : 201.88800

Appearance : Clear liquid

Melting point :−34 ℃(lit.) 

Boiling point: 167 ℃(lit.)

Relative density : 1.989 g/mL at 25 ℃(lit.)

Refractive index : n20/D 1.524(lit.)

Flash point :54 ℃

Content : ≥99.0%

Moisture : ≤0.05%

Other characters: 

Water Solvency: 1.7 g/L (30 ℃)  

Condition of storage:  The storage room is ventilated and dry and stored separately with food, oxidants and acids.

Stability:   Stable. Incompatible with strong oxidizing agents, strong bases. Flammable.

Purpose:Organic synthetic intermediates.

Packing:

250Kg / Iron drum

Structural formula:

Synthetic rout:

The product was prepared by the reaction of propanediol with bromohydrogen acid. Concentrated sulfuric acid and1,3-Propanediolwere added to the bromohydrogen acid, then slowly dripped into concentrated sulfuric acid, then refluxed in the sand bath for 7 hours, then the coarse product was steamed out and washed with water once. 10% sodium thiosulfate solution was used to wash 10% sodium carbonate twice for 2-3 times, then the water layer was removed and dried with anhydrous calcium chloride. The product was obtained by constant pressure fractionation and collection of 159-168 ℃ fractions.

UN No.:

UN 1993 3/PG 3

Packing group:

III

HS code:

2903399090