Items | Standard |
Appearance | Shallow pink to shallow brown crystalline powder |
Purity | ≥99.0% |
Initial melting point of dry product | ≥156.0 ℃ |
Phenol | ≤0.20% |
Ash specification | ≤0.30% |
Items | Standard |
Appearance | White blocky crystalline or crystalline powder, allowing a little yellow and light pink. |
Purity | ≥99.0% |
At the beginning of melting point | ≥158.0 ℃ |
Moisture content | ≤0.40% |
Phenol | ≤0.20% |
Easy carbon | Not deeper than 6 |
Dark spot | ≤12个/20 g |
Foreign matter | ≤5A/a |
Items | Standard | |
Appearance | White or Almost white crystalline powder or colourless acicular crystals | |
Solubility | Slightly soluble in water, freely soluble in ethanol (96 per cent), sparingly soluble in methylene chloride | |
IdentificationA.Melting point of salicylic acid | 158—161 ℃ | |
IdentificationB. IR-Spectrum | Should be complied with Reference Spectrum | |
Appearance of solution | Clear and colorless | |
Chloride | ≤100 ppm | |
Sulfate | ≤200 ppm | |
Heavy metals | ≤20 ppm | |
Loss on drying | ≤0.5% | |
Sulphated ash | ≤0.1% | |
Related substances | 4-hydroxybenzoic acid | ≤0.1% |
4-hydroxyisophthalic acid | ≤0.05% | |
Phenol | ≤0.02% | |
Other impurities | ≤0.05% | |
Total impurities | ≤0.2% | |
Assay | 99.0%—100.5% |
Items | Standard | |
Appearance and smell | White fine needle crystal or white crystalline powder; odorless or almost odorless | |
Solubility | Freely soluble in ethanol or ether, soluble in boiling water, sparingly soluble in chloroformslightly soluble in water | |
Melting point | 158~161 ℃ | |
Identification (1) Colorreaction | Violet color is produce | |
Identification(2)IR-Spectrum | Should be complied with Reference Spectrum (Spectral set 57) | |
Residue on ignition | ≤0.1% | |
Heavy metals | ≤10 ppm | |
Related substances | 4-hydroxybenzoic acid | ≤0.1% |
4-hydroxyisophthalic acid | ≤0.05% | |
Phenol | ≤0.02% | |
Other impurities | ≤0.05% | |
Total impurities | ≤0.2% | |
Assay | ≥99.5% |